发明授权
- 专利标题: Process for regenerating a zeolite catalyst
- 专利标题(中): 再生沸石催化剂的方法
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申请号: US776018申请日: 1991-10-15
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公开(公告)号: US5138108A公开(公告)日: 1992-08-11
- 发明人: Gerald C. Tustin , Joseph F. Jeter , Richard I. Garrity
- 申请人: Gerald C. Tustin , Joseph F. Jeter , Richard I. Garrity
- 申请人地址: NY Rochester
- 专利权人: Eastman Kodak Company
- 当前专利权人: Eastman Kodak Company
- 当前专利权人地址: NY Rochester
- 主分类号: C07B61/00
- IPC分类号: C07B61/00 ; B01J29/90 ; B01J38/64 ; C07C17/12 ; C07C17/156 ; C07C25/22
摘要:
Disclosed is a process for regeneration of a 13X zeolite catalyst comprising conducting the following steps within the regeneration zone wherein the 13X zeolite is located.(1) Applying vacuum or delivering a source of molecular oxygen or inert gas at a temperature above 100.degree. C. to remove a portion of the volatile compounds from the 13X zeolite,(2) Cooling the 13X zeolite to a temperature below 100 degrees C.,(3) Contacting the 13X zeolite with an aqueous solution having a pH in the range of 7 to 14,(4) Drying the 13X zeolite,(5) Delivering an oxygen containing calcination gas to the regeneration zone and heating the 13X zeolite to a temperature in the range of 350.degree. to 450.degree. C.,(6) Cooling the 13X zeolite to a temperature below 100 degrees C., and(7) Contacting the 13X zeolite with an aqueous solution having a pH in the range of 7 to 14.
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