发明授权
- 专利标题: Process for preparing high-purity aniline
- 专利标题(中): 制备高纯度苯胺的方法
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申请号: US896696申请日: 1992-06-10
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公开(公告)号: US5283365A公开(公告)日: 1994-02-01
- 发明人: Teruyuki Nagata , Katsuji Watanabe , Yoshitsugu Kono , Akihiro Tamaki , Takashi Kobayashi
- 申请人: Teruyuki Nagata , Katsuji Watanabe , Yoshitsugu Kono , Akihiro Tamaki , Takashi Kobayashi
- 申请人地址: JPX Tokyo
- 专利权人: Mitsui Toatsu Chemicals, Incorporated
- 当前专利权人: Mitsui Toatsu Chemicals, Incorporated
- 当前专利权人地址: JPX Tokyo
- 优先权: JPX3-123007 19900515
- 主分类号: C07C209/36
- IPC分类号: C07C209/36
摘要:
A process for the continuous preparation of aniline by hydrogenating nitrobenzene is disclosed which comprises the steps of suspending, in an aniline solvent, a catalyst of palladium or palladium-platinum which is deposited on a lipophilic carbon having an oil absorbency of at least 100, adding a zinc compound and an alkali metal carbonate or a zinc compound and an alkali metal bicarbonate as promotors to the reaction system, and carrying out reaction at a temperature of from 150 to 250.degree. C. substantially in the absence of water while aniline and water formed in said reaction are continuously distilled off as vapor from the reaction product, and the concentration of nitrobenzene in the reaction solution is maintained at 0.01% by weight or less.
公开/授权文献
- US5843515A Distributed control system for powder coating system 公开/授权日:1998-12-01
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