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US5354876A Preparation and purification of 1-amino-2-phenoxy-4-hydroxyanthraquinone 失效
1-氨基-2-苯氧基-4-羟基蒽醌的制备和纯化

Preparation and purification of 1-amino-2-phenoxy-4-hydroxyanthraquinone
摘要:
Pure 1-amino-2-phenoxy-4-hydroxyanthraquinone is prepared by reacting 1-amino-2-halo-4-hydroxyanthraquinone with phenol in aqueous suspension at pH 9-13 and 130.degree.-160.degree. C., adjusting the reaction mixture pH to 9.5-11.5 after the reaction has ended, separating the reaction product from the liquid phase, and ,washing it with alkaline hypochlorite solution.
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