发明授权
- 专利标题: Process for the production of polyether polyamines
- 专利标题(中): 聚醚多胺生产工艺
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申请号: US962223申请日: 1993-01-26
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公开(公告)号: US5371119A公开(公告)日: 1994-12-06
- 发明人: Ralf Bohlander , Guenter Uphues , Uwe Ploog
- 申请人: Ralf Bohlander , Guenter Uphues , Uwe Ploog
- 申请人地址: DEX Duesseldorf
- 专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人地址: DEX Duesseldorf
- 优先权: JPX2-01067 19900726
- 主分类号: A61K8/72
- IPC分类号: A61K8/72 ; A61K8/00 ; A61Q5/00 ; C08G65/32 ; C08G73/02 ; C08L63/00 ; C08K3/20
摘要:
A process for the preparation of polyether polyamines comprising the steps ofA) reacting a polyol with an epihalohydrin in the presence of a catalyst;B) adding an at least equimolar quantity of an aqueous alkali metal hydroxide, based on the weight of catalyst, to the reaction mixture formed in step A);C) distilling volatile constituents from the reaction mixture from step B) at a temperature below about 150.degree. C. and under a pressure below about 1.33.times.10.sup.4 Pa.;D) filtering the reaction mixture remaining after step C) at a temperature in the range of from about 80.degree. C. to about 100.degree. C. to remove insoluble components thereof from the bishalohydrin reaction product; andE) reacting the bishalohydrin reaction product with ammonia and/or an amine in the presence of an alkaline catalyst to form a polyether polyamine.
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