发明授权
- 专利标题: Preparation of diaryl carbonate
- 专利标题(中): 碳酸二芳基酯的制备
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申请号: US944251申请日: 1997-10-06
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公开(公告)号: US5792883A公开(公告)日: 1998-08-11
- 发明人: Katsumasa Harada , Ryoji Sugise , Koichi Kashiwagi , Takashi Doi , Sadao Niida , Toshio Kurafuji
- 申请人: Katsumasa Harada , Ryoji Sugise , Koichi Kashiwagi , Takashi Doi , Sadao Niida , Toshio Kurafuji
- 申请人地址: JPX Yamaguchi
- 专利权人: Ube Industries, Ltd.
- 当前专利权人: Ube Industries, Ltd.
- 当前专利权人地址: JPX Yamaguchi
- 优先权: JPX8-264765 19961004
- 主分类号: C07C68/00
- IPC分类号: C07C68/00
摘要:
An improved process for preparing a diaryl carbonate from a diaryl oxalate in a liquid phase by decarbonylation utilizes a reaction vessel composed of two or more reaction chambers which are connected in series. The process is composed of the steps of continuously introducing the diaryl oxalate and an organic phosphorus compound having a trivalent or pentavalent phosphorus atom and at least one carbon-phosphorus bonding into the first chamber and continuously recovering a reaction mixture mainly containing the diaryl carbonate from the last chamber under the condition that a mixture of the diaryl oxalate and the organic phosphorus compound is heated in the reaction chambers, while discharging carbon monoxide released from the mixture.
公开/授权文献
- US4805110A Circuit element mounting system and method 公开/授权日:1989-02-14