发明授权
- 专利标题: Process for the purification of glycidyl esters from epihalohydrin and carboxylic acids
- 专利标题(中): 从表卤代醇和羧酸纯化缩水甘油酯的方法
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申请号: US861408申请日: 1997-05-21
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公开(公告)号: US5880297A公开(公告)日: 1999-03-09
- 发明人: Richard William Ryan , Gerald G. McGlamery, Jr. , Ralph Martin Kowalik
- 申请人: Richard William Ryan , Gerald G. McGlamery, Jr. , Ralph Martin Kowalik
- 申请人地址: TX Houston
- 专利权人: Exxon Chemical Patents Inc.
- 当前专利权人: Exxon Chemical Patents Inc.
- 当前专利权人地址: TX Houston
- 主分类号: B01D3/00
- IPC分类号: B01D3/00 ; C07D301/32 ; C07D303/16
摘要:
A process for the distillation of the glycidyl ester reaction product of a straight or branched chain saturated monocarboxylic acid or salt thereof and an halo-substituted monoepoxidc is disclosed, wherein the reaction product is subjected to conditions of temperature and vacuum in a thin film, short pass distillation apparatus such as a wiped film evaporator. The product distillate has significantly reduced color than the reaction product prior to distillation, and has improved heat and color stability.
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