Invention Grant
- Patent Title: Process for the synthesis of flyash based Zeolite-A
- Patent Title (中): 用于合成基于飞灰的沸石-A的方法
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Application No.: US96821Application Date: 1998-06-12
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Publication No.: US5965105APublication Date: 1999-10-12
- Inventor: Sadhana Rayalu , Nitin Kumar Labhasetwar , Purushottam Khanna
- Applicant: Sadhana Rayalu , Nitin Kumar Labhasetwar , Purushottam Khanna
- Applicant Address: INX Rafimarg New Delhi
- Assignee: Council of Scientific and Industrial Research
- Current Assignee: Council of Scientific and Industrial Research
- Current Assignee Address: INX Rafimarg New Delhi
- Main IPC: C01B39/14
- IPC: C01B39/14
Abstract:
The present invention relates to a process for synthesis of flyash based Zeolite-A, said process comprising grinding and mixing of flyash and caustic soda in a ratio of 1:1.2 and optionally adding sodium aluminate or aluminium hydroxide to obtain a fine homogeneous fusion mixture; heating the said mixture in an inert vessel at about 500-600.degree. C. for about 1-2 hrs. to obtain a fused mass; cooling, milling, and mixing the said fused mass in distilled water for about 8-10 hrs. with simultaneous optional additon of sodium aluminate or alum solution, in the present or absence of NaC1 followed by optional addition of zeolite-A seeding to obtain amorphous alumino -silicate slurry; subjecting the said slurry to hydrothermal crystallisation at about 90-110.degree. C. for 2 to 4 hrs. to obtain Zeolite-A crystals; and washing the said crystals with water and then subjecting the washed crystals to oven drying at about 50-60.degree. C. to obtain the FAZ-A crystals.
Information query
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