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US6037489A Method of purifying glyoxylic esters and distillation equipment for purifying glyoxylic esters 失效
纯化乙醛酸酯的方法和纯化乙醛酸酯的蒸馏设备

Method of purifying glyoxylic esters and distillation equipment for
purifying glyoxylic esters
摘要:
A method for purifying glyoxylates includes (1) a coarse distillation process in which a crude glyoxylate in which water coexists is, in a film form, continuously subjected to coarse distillation, and (2) an azeotropic dehydration process in which the crude glyoxylate purified through the coarse distillation process is subjected to azeotropic dehydration in the presence of an azeotropic agent such as propyl acetate. By this method, high-purity glyoxylates can be efficiently and easily obtained at lower costs.
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