发明授权
US6043019A Robust method for the preparation of high bromide tabular grain emulsions 失效
制备高溴化物片状颗粒乳剂的稳健方法

Robust method for the preparation of high bromide tabular grain emulsions
摘要:
A method is disclosed of manufacturing a radiation-sensitive tabular grain emulsion comprised of (a) providing in a stirred reaction vessel a host tabular grain emulsion containing greater than 50 mole percent bromide, based on silver, and a speed enhancing amount of iodide and (b) then introducing a silver salt solution into the stirred reaction vessel, wherein (1) the silver salt solution is introduced into the stirred reaction vessel at a rate sufficient to create a new grain population, (2) halting introduction of the silver salt solution for a time sufficient to allow the new grain population to be ripened out, and (3) repeating steps (1) and (2) from 3 to 20 times until silver introduced in steps (1) and (2) amounts to from 5 to 50 percent of total silver forming the radiation-sensitive tabular grain emulsion.
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