Invention Grant
US06235866B1 Slurry preparation of bis (halophthalimides) and of polyether polymers
失效
双(卤代邻苯二酰亚胺)和聚醚聚合物的浆料制备
- Patent Title: Slurry preparation of bis (halophthalimides) and of polyether polymers
- Patent Title (中): 双(卤代邻苯二酰亚胺)和聚醚聚合物的浆料制备
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Application No.: US09413376Application Date: 1999-10-06
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Publication No.: US06235866B1Publication Date: 2001-05-22
- Inventor: Farid Fouad Khouri , Ganesh Kailasam , Joseph John Caringi , Peter David Phelps , Paul Edward Howson
- Applicant: Farid Fouad Khouri , Ganesh Kailasam , Joseph John Caringi , Peter David Phelps , Paul Edward Howson
- Main IPC: C08G802
- IPC: C08G802

Abstract:
Bis(halophthalimides) such as, 3-bis[N-(4-chlorophthalimido)]benzene are prepared in slurry in an organic liquid such as o-dichlorobenzene or anisole, by a reaction at a temperature of at least 150° C. between at least one diamino compound, preferably an aromatic diamine such as m- or p-phenylenediamine, and at least one halophthalic anhydride such as 4-chlorophthalic anhydride, in the presence of an imidization catalyst such as sodium phenylphosphinate. The solids content of the reaction mixture is at least about 5% and preferably at least about 12% by weight. The product slurry may be employed directly in the preparation of polyetherimides, and similar slurries may be employed to prepare other polyether polymers.
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