发明授权
- 专利标题: Process for producing &egr;-caprolactam
- 专利标题(中): 生产ε-己内酰胺的方法
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申请号: US09500997申请日: 2000-02-09
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公开(公告)号: US06265574B1公开(公告)日: 2001-07-24
- 发明人: Masaru Kitamura , Yasumoto Shimazu , Makoto Yako
- 申请人: Masaru Kitamura , Yasumoto Shimazu , Makoto Yako
- 优先权: JP11-031226 19990209
- 主分类号: C07D20104
- IPC分类号: C07D20104
摘要:
A process for producing &egr;-caprolactam is provided which comprises the steps of subjecting cyclohexanone oxime to a gaseous phase Beckmann rearrangement reaction in a fluidized bed system using a solid catalyst and re-generating the catalyst, wherein said process comprises a step of treating the catalyst with an oxygen-containing gas at an elevated temperature in a re-generation step so that the nitrogen content of the catalyst falls within a range of 10 ppm to 2,500 ppm on its way to the reaction step from the re-generating step. According to the present invention, &egr;-caprolactam is produced with a high conversion or a high selectivity without interrupting the rearrangement reaction or the re-generation step.
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