发明授权
US06307005B1 Robust process for the synthesis of polyestercarbonates 有权
用于合成聚酯碳酸酯的稳健工艺

Robust process for the synthesis of polyestercarbonates
摘要:
The present invention related to a method for preparing a polyestercarbonate, the method comprising: a) reacting a dihydric phenol and a diacid having from 12 to about 30 carbon atoms in the presence of an effective amount of carbonate precursor, thereby forming a reaction mixture, wherein the pH of the reaction mixture is maintained in an initial pH range of from about 8.5 to about 9.5 for about 50% to about 95% of the total carbonate precursor addition, and a second pH range of from about 10 to about 12 for the remainder of the carbonate precursor addition.
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