发明授权
- 专利标题: Method for producing camphorsultam
- 专利标题(中): 樟脑的生产方法
-
申请号: US09901077申请日: 2001-07-09
-
公开(公告)号: US06441187B1公开(公告)日: 2002-08-27
- 发明人: Hiroshi Shiratani , Shigeya Yamasaki
- 申请人: Hiroshi Shiratani , Shigeya Yamasaki
- 优先权: JP2000-253083 20000823
- 主分类号: C07D27506
- IPC分类号: C07D27506
摘要:
A method for producing camphorsultam, which includes the following steps 1 to 4: Step 1: reacting camphorsulfonic acid with a halogenation agent to give camphorsulfonyl halide, Step 2: reacting the camphorsulfonyl halide with ammonia to give camphorsulfonamide, Step 3: subjecting the camphorsulfonamide to dehydration and ring closure to give camphorsulfonimine, and Step 4: reducing the camphorsulfonimine with sodium borohydride in an aqueous isopropanol solution. According to this invention, camphorsultam and intermediates thereof can be obtained by an industrial method which is comparatively safe to the environment and human body, economical, and which is simple and easy.
公开/授权文献
- US20020091267A1 Method for producing camphorsultam 公开/授权日:2002-07-11
信息查询