发明授权
- 专利标题: Methods for the production of sulfurized diphenyloxides and compositions made therefrom
- 专利标题(中): 生产硫化二苯醚及其制备的组合物的方法
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申请号: US09473556申请日: 1999-12-29
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公开(公告)号: US06444623B1公开(公告)日: 2002-09-03
- 发明人: Margaret M. Wu , Philip Trotto , Rene B. LaPierre
- 申请人: Margaret M. Wu , Philip Trotto , Rene B. LaPierre
- 主分类号: C10M11102
- IPC分类号: C10M11102
摘要:
The present invention relates to methods for production of sulfurized diphenyloxides wherein a diphenyloxide is reacted with elemental sulfur in the presence of solid acid catalyst. The solid acid catalyst can be a zeolite or a catalytic amount of a Friedel-Crafts compound. The present invention further relates to a composition containing between about 40 and about 80 weight percent diphenyloxide; no more than about 15 weight percent diphenyloxide thiol; between about 5 and about 45 weight percent phenoxathiin; and between about 3 and about 50 weight percent total of bis(diphenyloxide) sulfide, diphenyloxide phenoxathiin sulfide, and bis(phenoxathiin) sulfide.