发明授权
- 专利标题: Methods for preparing phthalocyanine compositions
- 专利标题(中): 制备酞菁组合物的方法
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申请号: US10072237申请日: 2002-02-08
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公开(公告)号: US06476219B1公开(公告)日: 2002-11-05
- 发明人: James M. Duff , James D. Mayo , Roger E. Gaynor , Jeffrey H. Banning , Michael B. Meinhardt , Randall R. Bridgeman , Nan-Xing Hu , Carol A. Jennings , Marko D. Saban , Paul F. Smith , Hadi K. Mahabadi
- 申请人: James M. Duff , James D. Mayo , Roger E. Gaynor , Jeffrey H. Banning , Michael B. Meinhardt , Randall R. Bridgeman , Nan-Xing Hu , Carol A. Jennings , Marko D. Saban , Paul F. Smith , Hadi K. Mahabadi
- 主分类号: C07D48722
- IPC分类号: C07D48722
摘要:
Disclosed is a process for preparing a colorant of the formula wherein M is an atom or group of atoms capable of bonding to the central cavity of a phthalocyanine molecule, wherein axial ligands optionally can be attached to M, which comprises (a) reacting 3-n-pentadecylphenol with 4-nitrophthalonitrile in the presence of a base to form an alkylarylether adduct of phthalonitrile; and (b) reacting the alkylarylether adduct of phthalonitrile with either (i) a metal compound, or (ii) an ammonia-releasing compound in the presence of an alkanolamine solvent, or (iii) mixtures of (i) and (ii), to form the colorant.
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