- 专利标题: Method for producing xylylenediamine
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申请号: US09953557申请日: 2001-09-17
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公开(公告)号: US06476269B2公开(公告)日: 2002-11-05
- 发明人: Kenichi Nakamura , Susumu {overscore (O)}tsuka , Fumisada Kosuge , Takuji Shitara , Kazuhiko Amakawa
- 申请人: Kenichi Nakamura , Susumu {overscore (O)}tsuka , Fumisada Kosuge , Takuji Shitara , Kazuhiko Amakawa
- 优先权: JP2000-290459 20000925
- 主分类号: C07C21100
- IPC分类号: C07C21100
摘要:
A method for producing xylylenediamine by hydrogenating phthalonitrile synthesized through ammoxidation of xylene, wherein phthalonitrile is trapped in an organic solvent (A) by bringing a gas produced through ammoxidation into direct contact with the organic solvent (A), and hydrogenation including adding liquid ammonia to the resultant mixture is carried out without separation of phthalonitrile trapped in the organic solvent (A). Through this method, the phthalonitrile can be readily recovered from the produced gas and at high yield without need for new equipment, and xylylenediamine can be efficiently produced through hydrogenation. Xylylenediamine of high purity can be obtained by subjecting the produced xylylenediamine to extraction by use of an organic solvent (B) and water.
公开/授权文献
- US20020038054A1 Method for producing xylylenediamine 公开/授权日:2002-03-28
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