Invention Grant
- Patent Title: Method of preparing co-polymer particles
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Application No.: US09821034Application Date: 2001-03-30
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Publication No.: US06528582B2Publication Date: 2003-03-04
- Inventor: Kwok Tang , Guomin Bian , Leena Matilainen , Sinikka Ingelin
- Applicant: Kwok Tang , Guomin Bian , Leena Matilainen , Sinikka Ingelin
- Main IPC: C08L6124
- IPC: C08L6124

Abstract:
A one-step, in-situ, process for producing a high solids content emulsion or dispersion of partially or totally crosslinked urea formaldehyde (UF), melamine formaldehyde (MF), or melamine urea formaldehyde (MUF) resin droplets or particles, by forming a reaction mixture of (i) aqueous formaldehyde (formalin), (ii) at least one water-soluble protective colloid, (iii) water and (iv) optionally a surfactant, and mixing the reaction mixture in a reaction vessel; optionally adjusting the initial pH of the reaction mixture according to a desired value as needed; adding (i) urea or substituted urea, (ii) melamine or substituted melamine, or (iii) a mixture thereof, to the reaction mixture; and heating the reaction mixture to a temperature at which condensation takes place between the (i) urea or substituted urea, (ii) the melamine or substituted melamine, or (iii) the mixture thereof, and the formaldehyde to form a urea formaldehyde, melamine formaldehyde or melamine urea formaldehyde resin, and holding the reaction mixture at that temperature or a higher temperature, under mixing, for a period of time sufficient to achieve a desired degree of crosslinking in said urea formaldehyde, melamine formaldehyde or melamine urea formaldehyde resin; and cooling the reaction mixture. The droplet or particle size of the resulting resin dispersion can be controlled and adjusted by way of the present technique to the application requirements.
Public/Granted literature
- US20020004554A1 Method of preparing co-polymer particles Public/Granted day:2002-01-10
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