发明授权
- 专利标题: Method for purifying acrylic acid or methacrylic acid by crystallization and distillation
- 专利标题(中): 通过结晶和蒸馏纯化丙烯酸或甲基丙烯酸的方法
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申请号: US09719572申请日: 2001-01-02
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公开(公告)号: US06541665B1公开(公告)日: 2003-04-01
- 发明人: Erik Bastiaensen , Bernd Eck , Joachim Thiel
- 申请人: Erik Bastiaensen , Bernd Eck , Joachim Thiel
- 优先权: DE19829477 19980701
- 主分类号: C07C5143
- IPC分类号: C07C5143
摘要:
In a process for the purification of acrylic acid or methacrylic acid by crystallization and distillation, the following steps are carried out: (a) crystallization of a mixture containing the acrylic acid or methacrylic acid with formation of product crystals having a higher concentration of acrylic acid or methacrylic acid and of a mother liquor, (b) distillation of at least part of the mother liquor from step (a) with formation of a distillation residue, which is at least partly removed, and of a top product, (c) crystallization of at least part of the top product from step (b) with formation of a crystallization residue, which is removed, and of crystals and (d) recycling of the crystals from step (c) to the crystallization (a).
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