发明授权
- 专利标题: Method for producing α-hydroxycarboxylate
- 专利标题(中): α-羟基羧酸盐的制备方法
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申请号: US10680919申请日: 2003-10-08
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公开(公告)号: US07122698B2公开(公告)日: 2006-10-17
- 发明人: Hiroshi Yoshida , Hideaki Tsuneki , Toshio Hayashi , Hideyuki Baba , Takahiro Inagaki , Satoshi Nakagawa , Yukihiko Kakimoto , Ritsuo Kitada , Kohei Umehara
- 申请人: Hiroshi Yoshida , Hideaki Tsuneki , Toshio Hayashi , Hideyuki Baba , Takahiro Inagaki , Satoshi Nakagawa , Yukihiko Kakimoto , Ritsuo Kitada , Kohei Umehara
- 申请人地址: JP Osaka
- 专利权人: Nippon Shokubai Co., Ltd.
- 当前专利权人: Nippon Shokubai Co., Ltd.
- 当前专利权人地址: JP Osaka
- 代理机构: Knobbe, Martens, Olson & Bear LLP
- 优先权: JP2002-296621 20021009; JP2002-296623 20021009; JP2002-350987 20021203; JP2002-350994 20021203; JP2002-350997 20021203; JP2003-158809 20030604
- 主分类号: C07C69/66
- IPC分类号: C07C69/66
摘要:
The present invention provides a process for more efficiently producing an α-hydroxycarboxylic acid ester wherein side reactions due to the α-hydroxycarboxylic acid ester are inhibited or prevented in comparison with prior art production processes.The invention provides a process for producing an α-hydroxycarboxylic acid ester comprising Steps 1 to 3:Step 1. reacting, in the presence of oxygen, (i) a 1,2-diol with a 1,2-diol or (ii) a 1,2-diol with an alcohol to obtain a reaction product containing an α-hydroxycarboxylic acid ester;Step 2. separating the α-hydroxycarboxylic acid ester from the reaction product obtained in Step 1 by distillation under reduced pressure; andStep 3. feeding Step 1 with a mixture obtained by partially or entirely removing water from the reaction product, wherein the mixture contains an unreacted 1,2-diol and/or alcohol.
公开/授权文献
- US20050090686A1 Method for producing alpha - hydroxycarboxylate 公开/授权日:2005-04-28
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