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发明授权
US07132578B1 One-step synthesis of CF3-1 有权
一步合成CF3-1

One-step synthesis of CF3-1
摘要：
A process for the preparation of trifluoromethyl iodide is provided. The process includes the step of contacting in a reactor a compound represented by the formula: CF3—W and a compound represented by the formula: IFn wherein W can be H, Br, Cl, COOH, COCl, COOCH3, COOC2H5, COCH3, COPh, CF3, Si(CH3)3, SPh, SCH3, SSCF3, SSPh, SSCH3, or SO2Cl, wherein n is 1, 3, 5, or 7, and wherein the step of contacting is carried out, at a temperature, pressure and for a length of time sufficient to produce trifluoromethyl iodide. The contacting step can be carried out in the presence or absence of a catalyst and the contacting step can be carried out in the presence or absence of air.
摘要（中）：

提供了制备三氟甲基碘的方法。 该方法包括在反应器中接触由下式表示的化合物的步骤：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF 3 -W <？in-line-formula description =“In-line Formulas”end =“tail”？>和由下式表示的化合物：<？in-line-formula description =“In-line Formulas”end =“lead” 其中W可以是H，Br，Cl，COOH，COCl，COOCH CO 3，H 3，COCH 3，CO 2，CO 3，SO 3， 3，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个，3个， SUB或SO 2 Cl，其中n为1,3,5或7，并且其中接触步骤在温度，压力和时间长度下进行，足以 产生三氟甲基碘。 接触步骤可以在催化剂存在或不存在下进行，并且接触步骤可以在空气存在或不存在下进行。

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