发明授权
US07250080B1 Process for the manufacture of organosilicon compound-treated pigments
有权
用于制造有机硅化合物处理的颜料的方法
- 专利标题: Process for the manufacture of organosilicon compound-treated pigments
- 专利标题(中): 用于制造有机硅化合物处理的颜料的方法
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申请号: US11516157申请日: 2006-09-06
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公开(公告)号: US07250080B1公开(公告)日: 2007-07-31
- 发明人: Daniel H. Craig , Mark D. Westmeyer
- 申请人: Daniel H. Craig , Mark D. Westmeyer
- 申请人地址: US OK Oklahoma City
- 专利权人: Tronox LLC
- 当前专利权人: Tronox LLC
- 当前专利权人地址: US OK Oklahoma City
- 代理商 William B. Miller
- 主分类号: C09C3/12
- IPC分类号: C09C3/12 ; C09C1/36 ; B05D1/02 ; B05D3/02 ; B05D5/00
摘要:
An improved process for making an organosilicon compound surface-treated titanium dioxide material, comprising (a) forming a mixture of the titanium dioxide material in water, (b) wet milling the mixture, (c) adjusting the pH of the slurry resulting from step (b) to between about 5.0 and about 8.5, (d) after step (c), removing the titanium dioxide material from the mixture by vacuum or pressure filtration, (e) after step (d), washing the titanium dioxide material so removed, (f) after step (e), converting the washed titanium dioxide material to a fluid dispersion having a pH of from about 3.5 to less than about 7 via addition of a fluidizing agent comprising a water-soluble monoprotic acid, (g) after, or concurrently with, step (f), adding to the resulting dispersion of titanium dioxide material an organosilicon compound, with mixing, and (h) spray drying the dispersion of the washed titanium dioxide material resulting from step (g) to yield a dry titanium dioxide pigment powder.
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