发明授权
US07430871B2 NMR spectrometer with a common refrigerator for cooling an NMR probe head and cryostat
有权
NMR光谱仪,用于冷却NMR探针头和低温恒温器的普通冰箱
- 专利标题: NMR spectrometer with a common refrigerator for cooling an NMR probe head and cryostat
- 专利标题(中): NMR光谱仪,用于冷却NMR探针头和低温恒温器的普通冰箱
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申请号: US11266360申请日: 2005-11-04
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公开(公告)号: US07430871B2公开(公告)日: 2008-10-07
- 发明人: Marco Strobel
- 申请人: Marco Strobel
- 申请人地址: DE Rheinstetten
- 专利权人: Bruker Biospin GmbH
- 当前专利权人: Bruker Biospin GmbH
- 当前专利权人地址: DE Rheinstetten
- 代理商 Paul Vincent
- 优先权: DE102004053972 20041109
- 主分类号: F25B19/00
- IPC分类号: F25B19/00 ; B01D59/44 ; H01J49/40 ; H01F6/04
摘要:
An NMR spectrometer comprising a magnet coil system disposed in the helium tank (8) of a cryostat and an NMR probe head (4) which is disposed in a room temperature bore of the cryostat and contains a cooled RF resonator (13) for receiving NMR signals from a sample to be examined, wherein the helium tank (8) and the NMR probe head (4) are cooled by a common, multi-stage, compressor-operated refrigerator, is characterized in that the common refrigerator comprises a cold head (6) and several heat exchangers (21, 24, 25, 28, 31, 33, 34) at different temperature levels, wherein the refrigerator is disposed at a spatial separation from the cryostat in a separate, evacuated and thermally insulated housing (5), and several cooling circuits (1a, 1b, 1c, 1d, 2a, 2b, 3a, 3b) having thermally insulated transfer lines (14a, 14b, 15) are provided between the housing (5) containing the heat exchangers (21, 24, 25, 28, 31, 33, 34) and the cryostat, and also between the housing (5) and the NMR probe head (4). The probe head and magnet cryostat of the inventive NMR spectrometer can thereby be cooled by a common refrigerator, wherein the cooling resources of the used refrigerator are optimally utilized.
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