发明授权
- 专利标题: Method of producing xylylenediamine
- 专利标题(中): 产生苯二甲胺的方法
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申请号: US11749787申请日: 2007-05-17
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公开(公告)号: US07465832B2公开(公告)日: 2008-12-16
- 发明人: Tomohiro Sugawara , Takafumi Abe , Tatsuyuki Kumano , Kinji Kato
- 申请人: Tomohiro Sugawara , Takafumi Abe , Tatsuyuki Kumano , Kinji Kato
- 申请人地址: JP Tokyo
- 专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人地址: JP Tokyo
- 代理机构: Antonelli, Terry, Stout & Kraus, LLP.
- 优先权: JP2006-138812 20060518
- 主分类号: C07C209/48
- IPC分类号: C07C209/48
摘要:
A method of producing xylylenediamine of the present invention includes the steps of: subjecting a liquid mixture of phthalonitriles with liquid ammonia or a mixture of liquid ammonia and an organic solvent to a first catalytic hydrogenation treatment, thereby hydrogenating the phthalonitriles to obtain a reaction product (A), wherein a content of the liquid ammonia or the mixture of liquid ammonia and an organic solvent is 80 wt % or more; removing the liquid ammonia in the reaction product (A) to obtain a reaction product (B); subjecting the reaction product (B) to a second catalytic hydrogenation treatment, thereby hydrogenating cyanobenzylamine to obtain a reaction product (C); and distilling the reaction product (C) to purify xylylenediamine.
公开/授权文献
- US20070270613A1 METHOD OF PRODUCING XYLYLENEDIAMINE 公开/授权日:2007-11-22
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