发明授权
- 专利标题: Low water uptake silicas
- 专利标题(中): 低吸水二氧化硅
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申请号: US10500107申请日: 2002-12-24
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公开(公告)号: US07524478B2公开(公告)日: 2009-04-28
- 发明人: Remi Valero , Yvonick Chevallier
- 申请人: Remi Valero , Yvonick Chevallier
- 申请人地址: FR Aubervilliers
- 专利权人: Rhodia Chimie
- 当前专利权人: Rhodia Chimie
- 当前专利权人地址: FR Aubervilliers
- 代理机构: Buchanan, Ingersoll & Rooney P.C.
- 优先权: FR0116881 20011226
- 国际申请: PCT/FR02/04559 WO 20021224
- 国际公布: WO03/055801 WO 20030710
- 主分类号: C01B33/12
- IPC分类号: C01B33/12 ; C01B33/18 ; C01B33/187 ; C01B33/193
摘要:
The invention concerns a method for preparing low water uptake precipitated silicas, comprising successive steps which consist in: (a) producing an initial starter including a silicate, the silicate concentration in said starter, expressed in SiO2 equivalent, being less than 15 g/L; (b) bringing the medium pH to a value ranging between 7 and 8 by adding an acidifying agent, (c) in the resulting medium, simultaneously adding a silicate and an acidifying agent the respective amounts of silicate and acidifying agent added in time being specifically such that, during the entire addition (1) the reaction medium pH stays between 7 and 8, and (ii) the silicon concentration in the medium, expressed in SiO2 equivalent, stays below 35 g/L; (d) adding an acidifying agent in the medium resulting from step (c), so as to bring the medium to a pH ranging between 3 and 6.5; and (e) filtering the resulting aqueous silica dispersion, then drying the filter cake obtained at the end of the filtering step. The invention also concerns low water uptake silicas obtained by said method and their use, in particular for reinforcing silicones or polymer or elastomer matrices.
公开/授权文献
- US20050074386A1 Low water uptake silicas 公开/授权日:2005-04-07
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