发明授权
- 专利标题: Process for producing a high purity aromatic polycarboxylic acid
- 专利标题(中): 高纯度芳族多元羧酸的制备方法
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申请号: US10861497申请日: 2004-06-07
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公开(公告)号: US07547803B2公开(公告)日: 2009-06-16
- 发明人: Shinichi Nagao , Masato Inari , Jitsuo Oishi , Kenji Nakaya , Hiroshi Machida
- 申请人: Shinichi Nagao , Masato Inari , Jitsuo Oishi , Kenji Nakaya , Hiroshi Machida
- 申请人地址: JP Tokyo
- 专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人地址: JP Tokyo
- 代理机构: Antonelli, Terry, Stout & Kraus, LLP.
- 优先权: JP2003-176294 20030620
- 主分类号: C07C51/42
- IPC分类号: C07C51/42
摘要:
A process for producing a high purity aromatic polycarboxylic acid (APA) by purification of a crude APA comprises: (I) aging a slurry of the crude APA in a first dispersion medium at 180 to 300° C. for 10 minutes or longer under stirring; (II) introducing the aged slurry of the APA into a column for substituting dispersion media, bringing the slurry into contact with a second dispersion medium and separating the resultant fluid into a fluid of the first dispersion medium containing impurities and a slurry of the second dispersion medium containing crystals of the high purity APA; and (III) separating the crystals of the high purity APA from the slurry of the second dispersion medium. A high purity APA having excellent hue and particle diameter can be industrially advantageously produced while the construction of the process is simplified and the consumption of energy is decreased.
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