发明授权
- 专利标题: Method for obtaining crude 1,3-butadiene from a C4 fraction
- 专利标题(中): 从C4馏分获得粗1,3-丁二烯的方法
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申请号: US10557422申请日: 2004-05-19
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公开(公告)号: US07619126B2公开(公告)日: 2009-11-17
- 发明人: Bernd Heida
- 申请人: Bernd Heida
- 申请人地址: DE Ludwigshafen
- 专利权人: BASF Aktiengesellschaft
- 当前专利权人: BASF Aktiengesellschaft
- 当前专利权人地址: DE Ludwigshafen
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 优先权: DE10322655 20030520
- 国际申请: PCT/EP2004/005407 WO 20040519
- 国际公布: WO2004/103937 WO 20041202
- 主分类号: C07C7/08
- IPC分类号: C07C7/08 ; C07C11/167 ; B01D3/40 ; B01D3/42
摘要:
A process for recovering crude 1,3-butadiene from a C4 fraction by extractive distillation using a selective solvent in a dividing wall column (TK) in which a dividing wall (T) is arranged in the longitudinal direction of the column to form a first subregion (A), a second subregion (B) and a lower common column region (C) and which is preceded by an extractive scrubbing column (K), wherein the operation of the dividing wall column (TK) is set by regulation of the energy input into the dividing wall column (TK) via a bottom vaporizer (V) and setting of the number of the theoretical plates in the lower common column region (C) so that a bottom stream (17) consisting of purified solvent is obtained from the dividing wall column (TK), is proposed.
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