发明授权
US07622607B2 Method for purifying (meth)acrylic acid obtained by oxidizing a gaseous substrate 失效
纯化通过氧化气态基质得到的(甲基)丙烯酸的方法

  • 专利标题: Method for purifying (meth)acrylic acid obtained by oxidizing a gaseous substrate
  • 专利标题(中): 纯化通过氧化气态基质得到的(甲基)丙烯酸的方法
  • 申请号: US10577168
    申请日: 2004-10-01
  • 公开(公告)号: US07622607B2
    公开(公告)日: 2009-11-24
  • 发明人: Michel FauconetDenis Laurent
  • 申请人: Michel FauconetDenis Laurent
  • 申请人地址: FR Colombes
  • 专利权人: Arkema France
  • 当前专利权人: Arkema France
  • 当前专利权人地址: FR Colombes
  • 代理商 Steven D. Boyd
  • 优先权: FR0312906 20031104
  • 国际申请: PCT/FR2004/002481 WO 20041001
  • 国际公布: WO2005/054171 WO 20050616
  • 主分类号: C07C51/42
  • IPC分类号: C07C51/42
Method for purifying (meth)acrylic acid obtained by oxidizing a gaseous substrate
摘要:
The present invention relates to a method for purifying (meth)acrylic acid obtained by catalytic or redox oxidation of a gaseous substrate constituting propane, propylene, acrolein, isobutane, isobutene, tert-butyl alcohol and/or (meth)acrolein or mixtures thereof by sending the gaseous reaction mixture to the bottom of a countercurrent absorption column (C1) which is supplied at the top with at least one type of hydrophobic heavy solvent, sending the flow (4) from the bottom of column (C1) to a separation column (C2). Column (C1) is operated at a flow rate of heavy solvent of from 3 to 5.6 times the flow rate of the (meth)acrylic acid in the gaseous reaction mixture and the rectifying column used as a separation column (C2) is operated with the feed at the top and without reflux.
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