An amalgam separator for purifying a waste stream that contains a mixture of air and waste liquid. The amalgam separator contains filter media that comprises a sulfur-impregnated carrier and an ion exchange resin, wherein the ion exchange resin is present at a concentration of from about 25 to about 75 weight percent. During its operation, the amalgam separator separates the waste stream into air and waste liquid portions, purifies the waste liquid portion, and then combines the purified waste liquid portion with the air.