Invention Grant
- Patent Title: Method for producing electronic grade 2,2′-aminoethoxyethanol
- Patent Title (中): 生产电子级2,2'-氨基乙氧基乙醇的方法
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Application No.: US12443226Application Date: 2007-09-21
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Publication No.: US07825281B2Publication Date: 2010-11-02
- Inventor: Helmut Schmidtke , Martin Rudloff
- Applicant: Helmut Schmidtke , Martin Rudloff
- Applicant Address: DE Ludwigshafen
- Assignee: BASF Aktiengesellschaft
- Current Assignee: BASF Aktiengesellschaft
- Current Assignee Address: DE Ludwigshafen
- Agency: Connolly Bove Lodge & Hutz LLP
- Priority: EP06121405 20060928
- International Application: PCT/EP2007/060017 WO 20070921
- International Announcement: WO2008/037659 WO 20080403
- Main IPC: C07C209/16
- IPC: C07C209/16

Abstract:
A process for preparing electronics-grade 2,2′-aminoethyoxyethanol by reacting diethylene glycol with ammonia in the presence of a catalyst in a reactor to give a reaction mixture from which a crude 2,2′-aminoethoxyethanol stream is separated off and is purified further by distillation in a pure column, wherein a sidestream comprising electronics-grade 2,2′-aminoethoxyethanol is taken off from the pure column as a result of the diethylene glycol being passed through a filter which ensures a degree of removal of at least 99% for solid particles having a maximum particle size of ≦1.5 μm before the diethylene glycol is fed into the reactor, is proposed.
Public/Granted literature
- US20100029989A1 METHOD FOR PRODUCING ELECTRONIC GRADE 2,2'-AMINOETHOXYETHANOL Public/Granted day:2010-02-04
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