发明授权
- 专利标题: Method for producing dinitrotoluene
- 专利标题(中): 二硝基甲苯生产方法
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申请号: US10586683申请日: 2005-02-02
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公开(公告)号: US07851661B2公开(公告)日: 2010-12-14
- 发明人: Johannes Buettner , Wolfgang Mackenroth , Heinrich Hermann , Peter Konieczny , Juergen Gebauer
- 申请人: Johannes Buettner , Wolfgang Mackenroth , Heinrich Hermann , Peter Konieczny , Juergen Gebauer
- 申请人地址: DE Ludwigshafen
- 专利权人: BASF Aktiengesellschaft
- 当前专利权人: BASF Aktiengesellschaft
- 当前专利权人地址: DE Ludwigshafen
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 优先权: DE102004005913 20040205
- 国际申请: PCT/EP2005/001017 WO 20050202
- 国际公布: WO2005/075407 WO 20050818
- 主分类号: C07C205/00
- IPC分类号: C07C205/00
摘要:
The present invention provides a process for preparing dinitrotoluene, comprising the steps of a) reacting toluene with nitric acid in the presence of sulphuric acid to give mononitrotoluene, b) separating the reaction product from step a) into an organic phase comprising mononitrotoluene and an aqueous phase comprising sulfuric acid, c) reacting the organic phase comprising mononitrotoluene with nitric acid in the presence of sulphuric acid to give dinitrotoluene, d) separating the reaction product from step c) into an organic phase comprising dinitrotoluene and an aqueous phase comprising sulfuric acid, wherein the reaction product from step a) has a content of toluene of from 3.0 to 8% by weight, based on the organic phase, and a content of nitric acid of from 0.1 to 1.2% by weight, based on the aqueous phase, and the phase separation in step b) is effected in such a way that further reaction of the toluene with the nitric acid is prevented.
公开/授权文献
- US20080242900A1 Method for Producing Dinitrotoluene 公开/授权日:2008-10-02