发明授权
US07928370B2 Open probe method and device for sample introduction for mass spectrometry analysis
有权
用于质谱分析的样品引入的开放探针法和装置
- 专利标题: Open probe method and device for sample introduction for mass spectrometry analysis
- 专利标题(中): 用于质谱分析的样品引入的开放探针法和装置
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申请号: US12469779申请日: 2009-05-21
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公开(公告)号: US07928370B2公开(公告)日: 2011-04-19
- 发明人: Aviv Amirav , Alexander Gordin
- 申请人: Aviv Amirav , Alexander Gordin
- 申请人地址: IL Hod Hasharon
- 专利权人: Aviv Amirav
- 当前专利权人: Aviv Amirav
- 当前专利权人地址: IL Hod Hasharon
- 代理机构: Fleit Gibbons Gutman Bongini & Bianco PL
- 代理商 Martin Fleit; Paul D. Bianco
- 优先权: IL193003 20080723
- 主分类号: H01J49/26
- IPC分类号: H01J49/26 ; B01D53/02
摘要:
An open probe method for sample introduction into a mass spectrometer is disclosed, comprising the steps of: loading a sample holder with sample compounds to be analyzed; heating a probe oven; introducing said sample compounds in said sample holder into said heated probe oven; flowing inert gas into said heated probe oven; vaporizing said sample in said heated probe oven by the combined effect of oven temperature and inert gas flow; entraining said vaporized sample in said inert gas; and, transferring said vaporized sample in inert gas into an ion source of a mass spectrometer; wherein said heated probe oven remains open to the ambient atmosphere during sample introduction and analysis; said inert gas is flowing in said heated probe oven in two directions of a transfer line to a mass spectrometer ion source and to the oven opening; said vaporized sample in inert gas is transferred through a heated transfer line directly into the ionization chamber of an ion source of a mass spectrometer. An apparatus for this method of sample introduction is also disclosed. The primary advantage of this method and apparatus is that the heated probe oven remains open to the ambient atmosphere during sample introduction and analysis thereby enabling faster sample analysis.
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