发明授权
- 专利标题: Method for producing polymer beads of uniform size
- 专利标题(中): 生产尺寸均匀的聚合物珠粒的方法
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申请号: US12317768申请日: 2008-12-29
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公开(公告)号: US07947748B2公开(公告)日: 2011-05-24
- 发明人: John David Finch , Biwang Jiang , Aaron Sarafinas , Andrew M. Savo
- 申请人: John David Finch , Biwang Jiang , Aaron Sarafinas , Andrew M. Savo
- 申请人地址: US PA Philadelphia
- 专利权人: Rohm and Haas Company
- 当前专利权人: Rohm and Haas Company
- 当前专利权人地址: US PA Philadelphia
- 代理商 Kenneth Crimaldi
- 主分类号: B01J39/20
- IPC分类号: B01J39/20
摘要:
A method for preparing monodisperse crosslinked bead polymers by introducing droplets having a harmonic mean size from 50 to 1500 microns and comprising at least one monomer, at least one crosslinker and a free-radical polymerization initiator into an aqueous medium through orifices to produce an aqueous suspension of droplets having a volume fraction of droplets from 35 to 64%; wherein the droplets are not encapsulated; causing the aqueous suspension of droplets to flow in a downward direction in a pipe in which the temperature is maintained at least 20° C. below the temperature at which the polymerization initiator has a half-life of 1 hour; and polymerizing the droplets in a reactor.
公开/授权文献
- US20090176897A1 Method for producing polymer beads of uniform size 公开/授权日:2009-07-09
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