Invention Grant
- Patent Title: Process for operating a continuous removal of a target product X in the form of fine crystals of the target product X
- Patent Title (中): 用于以目标产物X的细晶体的形式连续移除靶产物X的方法
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Application No.: US12208559Application Date: 2008-09-11
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Publication No.: US08106240B2Publication Date: 2012-01-31
- Inventor: Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel
- Applicant: Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: DE102007043758 20070913
- Main IPC: C07C51/42
- IPC: C07C51/42

Abstract:
A process for operating a continuous removal of a target product X in the form of fine crystals of a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in the secondary chamber of an indirect heat exchanger to which liquid phase P flows continuously with simultaneous continuous flow through the primary chamber of the indirect heat exchanger with a coolant, and continuous withdrawal of a crystal suspension S having a degree of crystallization Y from the secondary chamber in two operating states I and II, wherein the coolant temperature is lower, the mass flow of liquid phase P is greater and the molar proportion of the constituents other than the target product X in the liquid phase P in operating state II is greater than in operating state I.
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