Invention Grant
- Patent Title: Method for preparing hydroxymethylfurfural
- Patent Title (中): 羟甲基糠醛的制备方法
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Application No.: US13346514Application Date: 2012-01-09
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Publication No.: US08455668B2Publication Date: 2013-06-04
- Inventor: Yao Fu , Jin Deng , Qingxiang Guo , Jing Zhao , Lei Liu
- Applicant: Yao Fu , Jin Deng , Qingxiang Guo , Jing Zhao , Lei Liu
- Applicant Address: CN
- Assignee: University of Science and Technology of China
- Current Assignee: University of Science and Technology of China
- Current Assignee Address: CN
- Agency: St. Onge Steward Johnston & Reens LLC
- Priority: CN200910150079 20090709
- Main IPC: C07D319/06
- IPC: C07D319/06

Abstract:
A method for preparing hydroxymethylfurfural, which includes: a) mixing and dissolving triose or its derivatives and solvent 1 to obtain the first reaction mixture; b) reacting the obtained first reaction mixture with Alkaline Catalyst 1 to condense into hexose; c) mixing and dissolving the resulting hexose and solvent 2 to obtain the second reaction mixture; d) adding acid catalyst 2 to the second reaction mixture, then heating the second reaction mixture at 80˜280° C. to form the third reaction mixture including hydroxymethylfurfural; e) obtaining the hydroxymethylfurfural separating by separating from the third mixture. The method is a new synthetic way for preparing 4-hydroxymethylfurfural and 5-hydroxymethylfurfural.
Public/Granted literature
- US20120172607A1 Method For Preparing Hydroxymethylfurfural Public/Granted day:2012-07-05
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