发明授权
- 专利标题: Process for starting up a separating process for purifying removal of acrylic acid crystals from a suspension S of crystals thereof in mother liquor
- 专利标题(中): 用于启动分离过程的方法,用于从母液中的晶体的悬浮液S中纯化除去丙烯酸晶体
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申请号: US12897199申请日: 2010-10-04
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公开(公告)号: US08461383B2公开(公告)日: 2013-06-11
- 发明人: Joerg Heilek , Dirk Litters , Klaus Joachim Mueller-Engel
- 申请人: Joerg Heilek , Dirk Litters , Klaus Joachim Mueller-Engel
- 申请人地址: DE Ludwigshafen
- 专利权人: BASF SE
- 当前专利权人: BASF SE
- 当前专利权人地址: DE Ludwigshafen
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 优先权: DE102009045767 20091016; DE102010030279 20100618
- 主分类号: C07C51/43
- IPC分类号: C07C51/43
摘要:
A process for starting up a separating process for purifying removal of acrylic acid crystals from a suspension S of crystals thereof in mother liquor with a hydraulic wash column which has a crystal melt circuit including crystal melt space, and a process space and a distributor space which are separated by an end with passages connecting the two spaces, in which the crystal bed is formed for the first time by first filling the crystal melt circuit and, at least partly, the process space with an acrylic acid-comprising startup liquid whose acrylic acid crystal formation temperature is less than or equal to the temperature of the suspension S increased by 15° C., and then continuing the filling of the wash column with the suspension S and optionally with control liquor until the difference between the pressure in the crystal melt space and the pressure in the distributor space falls suddenly, the arithmetic mean of the total waste liquor flow flowing through the filters of the filter tubes of the wash column until this time, based on the area of all filters, being not more than 80 m3/(m2·h).
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