Invention Grant
- Patent Title: Method for producing fluorine-containing polyether carboxylic acid amide
- Patent Title (中): 含氟聚醚羧酸酰胺的制造方法
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Application No.: US13265356Application Date: 2010-04-16
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Publication No.: US08476435B2Publication Date: 2013-07-02
- Inventor: Keisuke Kokin , Seiichiro Murata , Hideki Abe , Yusuke Takahashi
- Applicant: Keisuke Kokin , Seiichiro Murata , Hideki Abe , Yusuke Takahashi
- Applicant Address: JP Tokyo
- Assignee: Unimatec Co., Ltd.
- Current Assignee: Unimatec Co., Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Brinks Hofer Gilson & Lione
- Priority: JP2009-103036 20090421
- International Application: PCT/JP2010/056803 WO 20100416
- International Announcement: WO2010/122952 WO 20101028
- Main IPC: C07D239/02
- IPC: C07D239/02

Abstract:
A fluorine-containing polyether carboxylic acid amide represented by the general formula: CnF2n+1O(C3F6O)mRfCONHAr, wherein Rf is a fluorocarbon group having 1 to 2 carbon atoms, Ar is a nitrogen-containing heterocyclic group, n is an integer of 1 to 3, and m is an integer of 10 to 30, is produced by reacting a fluorine-containing polyether carboxylic acid fluoride represented by the general formula: CnF2n+1(C3F6O)mRfCOF, wherein Rf, n, and m are as defined above, with a nitrogen-containing heterocyclic amine compound represented by the general formula: ArNH2, wherein Ar is as defined above; wherein the reaction is carried out while a reaction temperature is first increased to 80 to 100° C., and then increased at a temperature increase rate that produces a temperature difference of 3 to 5° C. after 48 hours.
Public/Granted literature
- US20120041201A1 METHOD FOR PRODUCING FLUORINE-CONTAINING POLYETHER CARBOXYLIC ACID AMIDE Public/Granted day:2012-02-16
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