发明授权
- 专利标题: Process for preparing isocyanates in the gas phase
- 专利标题(中): 在气相中制备异氰酸酯的方法
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申请号: US13035166申请日: 2011-02-25
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公开(公告)号: US08487127B2公开(公告)日: 2013-07-16
- 发明人: Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
- 申请人: Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
- 申请人地址: DE Ludwigshafen
- 专利权人: BASF SE
- 当前专利权人: BASF SE
- 当前专利权人地址: DE Ludwigshafen
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 主分类号: C07C263/10
- IPC分类号: C07C263/10
摘要:
The invention relates to a process for preparing isocyanates by reacting the corresponding amines with phosgene in the gas phase, in the presence or absence of an inert medium, which comprises the following steps: (a) vaporization of the amine in a vaporizer, (b) superheating of the amine, (c) mixing of the gaseous amine with the phosgene and introduction into a reaction zone, (d) reaction of amine and phosgene to give isocyanate in the reaction zone, with a reaction mixture comprising isocyanate and hydrogen chloride being formed, (e) cooling of the reaction mixture comprising isocyanate and hydrogen chloride, wherein the vaporizer comprises a vessel in which tubes through which a heating medium flows are comprised, where number and diameter of the tubes are designed so that the tubes have a specific heat transfer area based on the volume through which the amine flows of at least 300 m2/m3.
公开/授权文献
- US20110213177A1 PROCESS FOR PREPARING ISOCYANATES IN THE GAS PHASE 公开/授权日:2011-09-01
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