发明授权
- 专利标题: Process for producing xylylenediamine
- 专利标题(中): 生产苯二甲胺的方法
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申请号: US13062334申请日: 2009-08-27
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公开(公告)号: US08759588B2公开(公告)日: 2014-06-24
- 发明人: Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
- 申请人: Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
- 申请人地址: JP Tokyo
- 专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人: Mitsubishi Gas Chemical Company, Inc.
- 当前专利权人地址: JP Tokyo
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 优先权: JP2008-230164 20080908
- 国际申请: PCT/JP2009/064989 WO 20090827
- 国际公布: WO2010/026920 WO 20100311
- 主分类号: C07C209/00
- IPC分类号: C07C209/00
摘要:
The invention provides a process for producing xylylenediamine, including supplying a solution of phthalonitrile dissolved in a solvent to a reactor filled with a catalyst and hydrogenating the phthalonitrile to produce xylylenediamine, characterized in that the process includes halting supply of the solution; (2) bringing a washing liquid into contact with the catalyst, the washing liquid having a phthalonitrile content of 3 mass % or less and a xylylenediamine content of 1 mass % or more; and after completion of the contact, resuming supply of the solution, and employing the catalyst continuously in hydrogenation. Through the production process of the invention, the catalyst can be employed continuously for a long period of time, and the catalyst-related cost can be considerably reduced.
公开/授权文献
- US20110245540A1 PROCESS FOR PRODUCING XYLYLENEDIAMINE 公开/授权日:2011-10-06
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