Invention Grant
- Patent Title: Catalyst composition and method for preparing amide using the same
- Patent Title (中): 催化剂组合物及其制备方法
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Application No.: US13332834Application Date: 2011-12-21
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Publication No.: US08865892B2Publication Date: 2014-10-21
- Inventor: Tung-Han Tsai , Cheng-Fa Hsieh , Hung-Hung Hseuh , Chien-Chuan Shih
- Applicant: Tung-Han Tsai , Cheng-Fa Hsieh , Hung-Hung Hseuh , Chien-Chuan Shih
- Applicant Address: TW Taipei
- Assignee: China Petroleum Development Corporation, Taipei (Taiwan)
- Current Assignee: China Petroleum Development Corporation, Taipei (Taiwan)
- Current Assignee Address: TW Taipei
- Agency: Edwards Wildman Palmer LLP
- Agent Peter F. Corless; Richard B. Emmons
- Priority: TW100101602A 20110117
- Main IPC: C07D201/04
- IPC: C07D201/04 ; B01J31/02 ; C07C231/10

Abstract:
The present invention provides a method for preparing an amide. The method includes the steps of performing in a reactor including a catalyst composition having a nitrogen-containing heterocyclic compound and sulfuric acid Beckman rearrangement of a ketoxime to form a product stream having the amide, wherein a molar ratio of the nitrogen-containing heterocyclic compound to the sulfuric acid is from 1:1 to 1:8; and separating an organic phase having the amide and an aqueous phase having the catalyst composition from the product stream. The present invention facilitates the regeneration of the catalyst composition with low water content, so as to increase the conversion rate of a ketoxime and the selectivity of an amide.
Public/Granted literature
- US20120184733A1 CATALYST COMPOSITION AND METHOD FOR PREPARING AMIDE USING THE SAME Public/Granted day:2012-07-19
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