发明授权
- 专利标题: Technological method for preparing sponge titanium from sodium fluotitanate raw material
- 专利标题(中): 从氟酸钠原料制备海绵钛的技术方法
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申请号: US13585783申请日: 2012-08-14
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公开(公告)号: US08871002B2公开(公告)日: 2014-10-28
- 发明人: Xuemin Chen , Jun Yang , Zhi Zhou
- 申请人: Xuemin Chen , Jun Yang , Zhi Zhou
- 申请人地址: CN Shenzhen, Guangdong
- 专利权人: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
- 当前专利权人: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
- 当前专利权人地址: CN Shenzhen, Guangdong
- 代理机构: Jackson IPG PLLC
- 优先权: CN201210014899 20120118
- 主分类号: C22B34/12
- IPC分类号: C22B34/12
摘要:
The invention provides a technological method for preparing sponge titanium from sodium fluotitanate raw material, comprising the following steps: step A: placing aluminum in an airtight resistance furnace, evacuating, introducing inert gas into the resistance furnace, and heating the aluminum to obtain molten aluminum; step B: opening a reactor cover, adding a proper amount of sodium fluotitanate into the reactor, closing the reactor cover, detecting leakage, slowly heating the reactor to 150° C., evacuating and continuously heating the reactor to 250° C.; step C: introducing inert gas into the reactor, continuously heating the reactor to 900° C., and stirring uniformly; step D: opening a valve, adjusting the stirring speed, dripping the molten aluminum, and controlling the temperature of reaction in a range from 900 to 1000° C.; and step E: opening the reactor cover, removing a stirring device out of the reactor, and eliminating NaAlF4 at upper layer to obtain sponge titanium.
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