Invention Grant
- Patent Title: Synthesis of high activity large crystal ZSM-5
- Patent Title (中): 高活性大晶体ZSM-5的合成
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Application No.: US13685794Application Date: 2012-11-27
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Publication No.: US08900547B2Publication Date: 2014-12-02
- Inventor: Wenyih Frank Lai , Merci A. Hamilton
- Applicant: ExxonMobil Research and Engineering Company
- Applicant Address: US NJ Annandale
- Assignee: ExxonMobil Research and Engineering Company
- Current Assignee: ExxonMobil Research and Engineering Company
- Current Assignee Address: US NJ Annandale
- Agent David M. Weisberg
- Main IPC: C01B39/38
- IPC: C01B39/38 ; B01J29/40 ; B01J35/02 ; C07C6/12

Abstract:
In a process for preparing a high activity, large crystal ZSM-5 type zeolite in the absence of a template, a reaction mixture can be prepared comprising water, a silica source having a surface area less than 150 m2/g, an alumina source, seeds, a source of an oxide of an alkali metal, M, and a source of gluconic acid or salt thereof, Q, wherein the mixture has a SiO2/Al2O3 molar ratio≦40. The reaction mixture can be heated to a crystallization temperature from about 100° C. to 200° C. for a time sufficient for crystals of ZSM-5 to form Crystals of ZSM-5 can then be recovered from the reaction mixture which crystals can have a SiO2/Al2O3 molar ratio≦40 and a majority of which crystals can have at least one crystalline dimension of at least about 2 μm.
Public/Granted literature
- US20130144100A1 SYNTHESIS OF HIGH ACTIVITY LARGE CRYSTAL ZSM-5 Public/Granted day:2013-06-06
Information query
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