Invention Grant
- Patent Title: Method for producing amide compound
- Patent Title (中): 酰胺化合物的制备方法
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Application No.: US14141916Application Date: 2013-12-27
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Publication No.: US08962826B2Publication Date: 2015-02-24
- Inventor: Junichi Kugimoto , Joji Kawai , Kazuo Yamato , Masahide Okada , Tsunemi Sugimoto , Hiroshi Matsumoto
- Applicant: Ube Industries, Ltd.
- Applicant Address: JP Ube-shi
- Assignee: Ube Industries, Ltd.
- Current Assignee: Ube Industries, Ltd.
- Current Assignee Address: JP Ube-shi
- Agency: Knobbe Martens Olson & Bear LLP
- Priority: JP2010-057123 20100315; JP2010-080851 20100331; JP2010-172322 20100730; JP2010-252108 20101110
- Main IPC: C07D225/02
- IPC: C07D225/02 ; C07D201/04 ; C07D201/06

Abstract:
A method for producing a high purity, high quality amide compound, particularly a lactam. An amount of each of a halide, an aldehyde compound, an alcohol compound and a nitrile compound contained in a solution recycled into an oxime-forming step is controlled to an amount of 0.4 mol% or less based on the ketone as a starting material. One or more of a ketone, an oxime and an amide compound are purified by hydrogenation and/or crystallization for eliminating impurities containing a double bond. A content of impurities having a cyclic bridge structure is controlled using a cycloalkanone purified by recrystallization.
Public/Granted literature
- US20140114062A1 METHOD FOR PRODUCING AMIDE COMPOUND Public/Granted day:2014-04-24
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