发明授权
US09085506B2 Process for preparing 3-aminomethyl-3,5,5-trimethylcyclohexylamine
有权
3-氨基甲基-3,5,5-三甲基环己胺的制备方法
- 专利标题: Process for preparing 3-aminomethyl-3,5,5-trimethylcyclohexylamine
- 专利标题(中): 3-氨基甲基-3,5,5-三甲基环己胺的制备方法
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申请号: US13991718申请日: 2011-11-18
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公开(公告)号: US09085506B2公开(公告)日: 2015-07-21
- 发明人: Markus Galle , Gerda Grund , Axel Hengstermann , Michael D Hinton , Rolf Hirsch , Robert Jansen , Cord Knoop , Christian Lettmann , Juergen Lippe , Martin Maier , Joerg-Joachim Nitz , Matthias Orschel , Martina Ortelt , Norbert Richter , Armin Rix , Markus Schwarz , Guido Streukens
- 申请人: Markus Galle , Gerda Grund , Axel Hengstermann , Michael D Hinton , Rolf Hirsch , Robert Jansen , Cord Knoop , Christian Lettmann , Juergen Lippe , Martin Maier , Joerg-Joachim Nitz , Matthias Orschel , Martina Ortelt , Norbert Richter , Armin Rix , Markus Schwarz , Guido Streukens
- 申请人地址: DE Essen
- 专利权人: Evonik Degussa GmbH
- 当前专利权人: Evonik Degussa GmbH
- 当前专利权人地址: DE Essen
- 代理机构: Oblon, McClelland, Maier & Neustadt, L.L.P.
- 优先权: DE102010062603 20101208
- 国际申请: PCT/EP2011/070442 WO 20111118
- 国际公布: WO2012/076317 WO 20120614
- 主分类号: C07C209/00
- IPC分类号: C07C209/00 ; C07C209/48 ; C07C209/26 ; C07C253/10 ; C07C45/74
摘要:
The invention relates to an improved process for preparing 3-aminomethyl-3,5,5-trimethylcyclohexylamine, referred to hereinafter as isophoronediamine or, in abbreviated form, IPDA, by: I. preparation of isophorone by catalyzed aldol condensations with acetone as reactant; II. reaction of isophorone with HCN to form isophoronenitrile (IPN, 3-cyano-3,5,5-trimethylcyclohexanone); III. catalytic hydrogenation and/or catalytic reductive amination (also referred to as aminative hydrogenation) of 3-cyano-3,5,5-trimethylcyclohexanone, hereinafter called isophoronenitrile or, in abbreviated form, IPN, to give the isophoronediamine.
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