Invention Grant
- Patent Title: Method for purifying vanillin by liquid-liquid extraction
- Patent Title (中): 通过液 - 液萃取纯化香草醛的方法
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Application No.: US14364316Application Date: 2012-12-13
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Publication No.: US09126917B2Publication Date: 2015-09-08
- Inventor: Martine Vibert , Corine Cochennec , Alain Etchebarne
- Applicant: RHODIA OPERATIONS
- Applicant Address: FR Paris
- Assignee: RHODIA OPERATIONS
- Current Assignee: RHODIA OPERATIONS
- Current Assignee Address: FR Paris
- Priority: FR1161681 20111215
- International Application: PCT/EP2012/075456 WO 20121213
- International Announcement: WO2013/087795 WO 20130620
- Main IPC: C07C45/80
- IPC: C07C45/80

Abstract:
A method is described for purifying vanillin, and derivatives thereof, from an initial solution of vanillin or of a vanillin derivative in a solvent S1 containing impurities, comprising the following steps: a) a step of evaporating the solvent S1 in the presence of water from such initial solution to obtain an aqueous solution of vanillin or of a vanillin derivative; b) a step of liquid/liquid extraction by bringing the aqueous solution obtained at the end of step a) into contact with a solvent S2, at a pH of greater than 8 and less than 10, to obtain an organic phase and an aqueous phase containing vanillin or a vanillin derivative and residual solvent S2; c) a step of precipitating, at a pH between 4 and 7.5, the vanillin contained in the aqueous phase obtained at the end of step b); and d) a step of isolating the vanillin or derivative thereof.
Public/Granted literature
- US20140316165A1 Method for purifying vanillin by liquid-liquid extraction Public/Granted day:2014-10-23
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