Invention Grant
US09126917B2 Method for purifying vanillin by liquid-liquid extraction 有权
通过液 - 液萃取纯化香草醛的方法

  • Patent Title: Method for purifying vanillin by liquid-liquid extraction
  • Patent Title (中): 通过液 - 液萃取纯化香草醛的方法
  • Application No.: US14364316
    Application Date: 2012-12-13
  • Publication No.: US09126917B2
    Publication Date: 2015-09-08
  • Inventor: Martine VibertCorine CochennecAlain Etchebarne
  • Applicant: RHODIA OPERATIONS
  • Applicant Address: FR Paris
  • Assignee: RHODIA OPERATIONS
  • Current Assignee: RHODIA OPERATIONS
  • Current Assignee Address: FR Paris
  • Priority: FR1161681 20111215
  • International Application: PCT/EP2012/075456 WO 20121213
  • International Announcement: WO2013/087795 WO 20130620
  • Main IPC: C07C45/80
  • IPC: C07C45/80
Method for purifying vanillin by liquid-liquid extraction
Abstract:
A method is described for purifying vanillin, and derivatives thereof, from an initial solution of vanillin or of a vanillin derivative in a solvent S1 containing impurities, comprising the following steps: a) a step of evaporating the solvent S1 in the presence of water from such initial solution to obtain an aqueous solution of vanillin or of a vanillin derivative; b) a step of liquid/liquid extraction by bringing the aqueous solution obtained at the end of step a) into contact with a solvent S2, at a pH of greater than 8 and less than 10, to obtain an organic phase and an aqueous phase containing vanillin or a vanillin derivative and residual solvent S2; c) a step of precipitating, at a pH between 4 and 7.5, the vanillin contained in the aqueous phase obtained at the end of step b); and d) a step of isolating the vanillin or derivative thereof.
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