发明授权
- 专利标题: Polyacrylic acid (salt)-type water absorbent resin and method for producing of same
- 专利标题(中): 聚丙烯酸(盐)型吸水性树脂及其制造方法
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申请号: US13392256申请日: 2010-08-27
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公开(公告)号: US09138505B2公开(公告)日: 2015-09-22
- 发明人: Kozo Nogi , Kunihiko Ishizaki , Katsuyuki Wada
- 申请人: Kozo Nogi , Kunihiko Ishizaki , Katsuyuki Wada
- 申请人地址: JP Osaka
- 专利权人: NIPPON SHOKUBAI CO., LTD.
- 当前专利权人: NIPPON SHOKUBAI CO., LTD.
- 当前专利权人地址: JP Osaka
- 代理机构: Roylance, Abrams, Berdo & Goodman, L.L.P.
- 优先权: JP2009-196967 20090827; JP2009-197022 20090827; JP2009-197063 20090827; JP2009-197091 20090827
- 国际申请: PCT/JP2010/064641 WO 20100827
- 国际公布: WO2011/024971 WO 20110303
- 主分类号: C08F20/02
- IPC分类号: C08F20/02 ; A61L15/24 ; C08J3/24 ; A61L15/60 ; C08F120/06 ; C08F220/06
摘要:
Disclosed is a method for producing a water absorbent resin, by which a surface-crosslinked water absorbent resin having excellent physical properties can be efficiently obtained at low cost, while assuring high productivity. When the production scale is increased to a continuous production on a huge scale (for example, 1 t/hr or more), the physical properties are improved and stabilized (for example, standard deviation of the physical properties is reduced) by a surface-crosslinking treatment, and the absorption against pressure (AAP) and liquid permeability (SFC) are further improved. Specifically disclosed is a method for continuously producing a polyacrylic acid (salt)-type water absorbent resin powder, which comprises: a step of preparing an aqueous monomer solution using an acrylic acid (salt); a step of polymerizing the aqueous monomer solution; a shredding step of a hydrous gel-like crosslinked polymer during or after the polymerization; a step of drying the thus-obtained particulate hydrous gel-like crosslinked polymer; a step of crushing and classifying the dried product; a step of heating and surface-crosslinking after the classification; and a step of cooling after the surface-crosslinking. In the method for producing a polyacrylic acid (salt)-type water absorbent resin, the internal area of the cooling device that is used in the cooling step is 0.25-0.95 times the internal area of the heating device that is used in the surface-crosslinking step.
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