发明授权
- 专利标题: Method for concentrating an aqueous hydrogen peroxide solution
- 专利标题(中): 浓缩过氧化氢水溶液的方法
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申请号: US13817797申请日: 2011-07-29
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公开(公告)号: US09206047B2公开(公告)日: 2015-12-08
- 发明人: Hubertus Eickhoff , Florian Lode , Eduardo Arevalo , Marc Brendel , Claudia Wallert
- 申请人: Hubertus Eickhoff , Florian Lode , Eduardo Arevalo , Marc Brendel , Claudia Wallert
- 申请人地址: DE Essen
- 专利权人: Evonik Degussa GmbH
- 当前专利权人: Evonik Degussa GmbH
- 当前专利权人地址: DE Essen
- 代理机构: Law Office of: Michael A. Sanzo, LLC
- 优先权: DE102010039748 20100825
- 国际申请: PCT/EP2011/063069 WO 20110729
- 国际公布: WO2012/025333 WO 20120301
- 主分类号: C01B15/013
- IPC分类号: C01B15/013 ; B01D1/28 ; B01D3/14 ; B01D3/42 ; C01B15/037
摘要:
The invention is directed to a process for concentrating aqueous hydrogen peroxide solution to give at least two hydrogen peroxide streams of different concentration in an apparatus which includes a preevaporator (1), a distillation column (2) and a vapour compressor (3). The aqueous hydrogen peroxide solution to be concentrated (4) is continuously fed into the preevaporator; vapour (5) produced by evaporation in the preevaporator is fed to the distillation column; bottom product (6) obtained in the preevaporator is withdrawn as a first concentrated hydrogen peroxide stream (7); vapour (8) produced in the distillation column is withdrawn from the distillation column at the top of the column, compressed by the vapour compressor and used for heating the preevaporator; and the bottom product (9) obtained in the distillation column is withdrawn as a second concentrated hydrogen peroxide stream (10); Concentrated hydrogen peroxide solutions having differing concentrations in the range from 50 to 70% by weight of hydrogen peroxide can be produced at the same time in a freely selectable ratio by feeding part of the bottom product obtained in the preevaporator in liquid form to the distillation column.
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