发明授权
- 专利标题: Reactor for liquid phase fluorination reactions
- 专利标题(中): 反应器用于液相氟化反应
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申请号: US14618500申请日: 2015-02-10
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公开(公告)号: US09353028B2公开(公告)日: 2016-05-31
- 发明人: Daniel C. Merkel , Barry Asher Mahler , Hsueh Sung Tung , Mario Joseph Nappa
- 申请人: HONEYWELL INTERNATIONAL INC.
- 申请人地址: US NJ Morristown
- 专利权人: HONEYWELL INTERNATIONAL INC.
- 当前专利权人: HONEYWELL INTERNATIONAL INC.
- 当前专利权人地址: US NJ Morristown
- 代理机构: Scully Scott Murphy and Presser
- 主分类号: C07C17/087
- IPC分类号: C07C17/087 ; C07C17/20 ; B01J19/18 ; C07C17/25
摘要:
The present invention relates to a hydrofluorinating process which comprises reacting a fluoroolefin with hydrogen fluoride in the liquid phase in the presence of a hydrofluorination catalyst in the reaction zone of a reactor, said reactor comprised of a reactor body having a length to diameter ratio of about 2:1 or greater; a stirred reaction zone containing said hydrofluorination catalyst, which may be prepared in situ, at least one inlet for supplying said hydrogen fluoride and fluoroolefin to the reaction zone and at least one outlet for recovering said fluoroalkane, said stirrer disposed in the reaction zone and comprising a plurality of blades fixedly attached to shaft drivable by a motor, said blades extending from about the bottom of the reaction zone to about the top of the reaction zone and said shaft extending on a longitudinal axis from the bottom of the reactor to the top of the reactor, said stirrer being rotated at a speed sufficient to promote a swirling of the liquid to effect the occurrence of hydrofluorination reaction and minimize overfluorination. The present invention also relates to said hydrofluorination reactor.
公开/授权文献
- US20150225316A1 REACTOR FOR LIQUID PHASE FLUORINATION REACTIONS 公开/授权日:2015-08-13
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