- 专利标题: Method for producing metal hydride
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申请号: US15021533申请日: 2014-09-25
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公开(公告)号: US09650247B2公开(公告)日: 2017-05-16
- 发明人: Tetsuya Ishimoto , Shoji Suzuki , Katsumi Matsui , Tomoki Hatsumori , Kazuhiko Tokoyoda
- 申请人: TAIHEIYO CEMENT CORPORATION
- 申请人地址: JP Minato-ku
- 专利权人: TAIHEIYO CEMENT CORPORATION
- 当前专利权人: TAIHEIYO CEMENT CORPORATION
- 当前专利权人地址: JP Minato-ku
- 代理机构: Oblon, McClelland, Maier & Neustadt, L.L.P.
- 优先权: JP2013-198185 20130925
- 国际申请: PCT/JP2014/075348 WO 20140925
- 国际公布: WO2015/046284 WO 20150402
- 主分类号: C01B6/04
- IPC分类号: C01B6/04 ; C01B6/02
摘要:
A method for efficiently producing a high-purity metal hydride without contamination of other metals while initiating reaction rapidly is provided.A method for producing a metal hydride from a metal selected from the group consisting of Group 2 metals and Group 3 metals comprising: (A) charging the pressure resistant container with the metal, introducing hydrogen into the container, and heating the container to initiate reaction, wherein a gauge pressure (a) is set to 0.1 to 1.5 MPa, a heating temperature (b) is set to 50 to 250° C., and a product of the gauge pressure and the heating temperature, a×b, is set in the range of 20 to 100; (B) stopping the introduction of hydrogen to allow the reaction to proceed when the temperature in the reaction container is increased to a temperature higher by 10 to 100° C. than the heating temperature; (C) introducing hydrogen of 0.1 to 1.5 MPa to allow the reaction to proceed when the temperature in the reaction container is decreased to the temperature at which the introduction of the hydrogen has been stopped; and (D) repeating the steps (B) and (C) until an increase in temperature does not occur in the reaction container after the introduction of the hydrogen.
公开/授权文献
- US20160244328A1 METHOD FOR PRODUCING METAL HYDRIDE 公开/授权日:2016-08-25
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