Invention Grant
- Patent Title: Process for the synthesis of 3-methyl-pyridine
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Application No.: US12822770Application Date: 2010-06-24
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Publication No.: US09701634B2Publication Date: 2017-07-11
- Inventor: Detlef Roederer , Daniel Zollinger , Jean-Yves De Riedmatten
- Applicant: Detlef Roederer , Daniel Zollinger , Jean-Yves De Riedmatten
- Applicant Address: CH Basel
- Assignee: LONZA LTD
- Current Assignee: LONZA LTD
- Current Assignee Address: CH Basel
- Agency: Hoffmann & Baron, LLP
- Priority: EP09008251 20090624
- Main IPC: C07D213/10
- IPC: C07D213/10

Abstract:
The present invention discloses a process for the synthesis of 3-methyl-pyridine from formaldehyde, paracetaldehyde, ammonia and acetic acid, whereby said compounds are reacted and said process comprises the following parameters: a) a reaction temperature of 260-300° C.; b) a molar ratio of formaldehyde and paraldehyde (calculated as acetaldehyde) of 0.7-1.4 mol/mol: c) an ammonia concentration of 10-20 weight-% d) an acetic acid concentration of 4-20 weight-% e) a paraldehyde (calculated as acetaldehyde) concentration of 0.4-1.6 Mol/kg f) a retention time of 10-30 minutes in case of a continuous reaction and 10-90 minutes in case of a discontinuous reaction; and g) a reaction pressure of 30-130 bar.
Public/Granted literature
- US20110003997A1 Process for the synthesis of 3-methyl-pyridine Public/Granted day:2011-01-06
Information query
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