Invention Grant
- Patent Title: Method for preparing cellulose nanofiber capable of being stably dispersed
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Application No.: US14361861Application Date: 2012-11-06
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Publication No.: US09725583B2Publication Date: 2017-08-08
- Inventor: Min Wu , Yong Huang , Shigenori Kuga , Pei Huang
- Applicant: Technical Institute of Physics and Chemistry of the Chinese Academy of Sciences
- Applicant Address: CN Beijing
- Assignee: Technical Institute of Physics and Chemistry of the Chinese Academy of Sciences
- Current Assignee: Technical Institute of Physics and Chemistry of the Chinese Academy of Sciences
- Current Assignee Address: CN Beijing
- Agency: Eversheds Sutherland (US) LLP
- Priority: CN201110391262 20111130
- International Application: PCT/CN2012/084128 WO 20121106
- International Announcement: WO2013/078936 WO 20130606
- Main IPC: C08L1/12
- IPC: C08L1/12 ; D01F2/28 ; C08B3/00 ; C08B3/20 ; C08B16/00 ; C08L1/10

Abstract:
A method for preparing stably dispersed cellulose nanofibers comprises the following steps: 1) mixing cellulose and an organic solvent, the percentage of the cellulose being 1% to 15% in weight; 2) adding an esterification agent into the resultant mixture of step 1), the molar ratio of the esterification agent to the cellulose being from 1:0.1 to 4; and 3) physically breaking the resultant mixture of step 2) until a suspension liquid with stably dispersed cellulose nanofibers of 2-1000 nm in diameter and 10-100 μm in length is obtained, an esterification reaction of hydroxyl group(s) on the surface of cellulose fibers occurring at the time of the breaking. Also disclosed are dispersed cellulose nanofibers with improved compatibility to the matrix than the untreated cellulose and an improved strength of the composite materials.
Public/Granted literature
- US20140299019A1 Method for Preparing Cellulose Nanofiber Capable of Being Stably Dispersed Public/Granted day:2014-10-09
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